Octamethyl-21, 22, 23, 24-tetroxaquaterene was synthesized by the condensation of furan with acetone using 2-methoxyethanol as solvent in the presence of Mg(ClO4)2 and hydrochloric.
本文以乙二醇独甲醚作溶剂,在Mg(CIO4)2及盐酸存在下,使呋喃和丙酮缩合,合成了 2,2,7,7,12,12,17,17-八甲基-21,22,23,24-四氧夸哒烯,产率达39%~54%