1) The free radical polymerization of styrene initiated with azobis(isobutyronitrile) in the presence of benzene sulfonyl chloride (BSC) was carried out.
本论文以磺酰氯为基础，进行了多方面的研究，包括其链转移反应的研究，在制备支化聚合物和接枝聚合物方面的应用，具体工作如下： 1)首先以偶氮二异丁腈为自由基引发剂，苯磺酰氯存在下进行苯乙烯的自由基聚合。
A variety of synthetic methods of sulfonyl chloride were reviewed with 49 references,including chlorosulfonation with chlorosulfonic acid,chlorination of sulfonic acid,oxidation and chlorination of sulfide,diazotization and chlorosulfonation of compounds with amino group,indirect chlorosulfonation of halide and chlorosulfonation of alkane.
综述了磺酰氯的合成方法,主要包括氯磺酸直接氯磺化,由磺酸氯化、含硫化合物氧化并氯化、由氨基化合物经重氮化并氯磺化、由卤代物间接氯磺化和饱和烷烃直接氯磺化等,并对各种合成方法的要点和适用范围等进行了评述。
Hydrocarbyl sulfuryl chloride was prepared by the oxidation of S - hydrocarbyl isothiouronium salts, thiocyanic esters and sulfuric ether in the medium of hydrochloric acid under mild conditions with high yields.
以S-烃基异硫脲盐、硫氰酸酯、硫醚为底物,在盐酸介质中,温和条件下,通过氧化法高产率地合成了烃基磺酰氯;探讨了氧化剂作用机理;合成中采用PTC技术,使产品收率可提高30％。
Synthesis of dansyl chloride allylamine;
丹磺酰氯烯丙基胺的制备
Study on derivatising condition of biogenic amines with dansyl chloride as pre-column derivatising agent;
丹磺酰氯作为生物胺柱前衍生试剂衍生化条件的研究
Labellized by dansyl chloride,17β-estradiol has been synthesized into fluorescent analyte successfully.
采用分子印迹技术,通过丹磺酰氯与17β-雌二醇反应,合成出17β-雌二醇荧光标记物;建立了微球法合成17β-雌二醇荧光标记化合物分子印迹微球聚合物的方法,所获得的微球粒径均匀,平均为300~400 nm;分子印迹微球聚合物在不同极性溶剂中对17β-雌二醇荧光标记化合物的结合常数顺序为乙腈>甲醇>水>二氯甲烷,其结合量的差异并不显著,平均值为9。
Study on addition reaction of benzenesulfonyl chloride and isoprene;
苯磺酰氯和异戊二烯加成反应研究
In this improved technology,the yield of benzenesulfonyl chloride was raised from 80.
以苯为原料 ,合成了苯磺酰氯。
Novel phenylsulfonylurea derivatives were synthesized by the reaction of 1-[(6-chloro-3- pyridyl)methyl]-2-imidazolidone with benzenesulfonyl chlorides and structurally characterized by IR, 1H NMR, 13C NMR techniques and elemental analysis.
以2-氯-5-氯甲基吡啶和不同取代基的苯磺酰氯为原料,合成了7个新型的苯磺酰内脲类衍生物,并用FT-IR,1HNMR,13CNMR,元素分析对其结构进行了表征,同时对合成目标化合物的反应条件进行了探究。
para-acetamidobenzene sulfonyl chloride
对乙酰氨基苯磺酰氯
Determination of Taurine in Food by Pre-column HPLC with Sulfonyl Chloride;
应用单磺酰氯柱前衍生法测定食品中的牛磺酸
A Study on Green Synthesis of 3-Nitrobenzenesulfonyl Chloride
间硝基苯磺酰氯绿色合成新技术研究
Synthesis of biphenyl-4,4′-disulfonyl chloride under microwave irradiation
微波法合成4,4′-联苯二磺酰氯
A New Method of Structral Confirmation of Chlorosulfonyl-Containing Azo Compounds
磺酰氯化合物结构表征的一种新方法
Dri-sol process
德里索防缩法（用磺酰氯进行羊毛氯化防缩法）
Preparation of Polystyrylsulfonyl Chloride Resin and Its Application in Synthesis of Nitrogen-Containing Basic Resins
聚苯乙烯磺酰氯树脂的制备及其在含氮碱性树脂合成中的应用
Atom Transfer Radical Polymerization Initiated by Dodecyl Benzene Sulfonyl Chlorine;
十二烷基苯磺酰氯引发的原子转移自由基聚合研究
Preparation of Functional Film on Dansyl Chloride as Fluorescence Probe;
以5-二甲氨基萘磺酰氯为荧光探针的功能膜制备
Study on the Function Group Uniformity of Polystyrol Sulfonyl Chloride Resins by Infrared Spectra
红外光谱法研究聚苯乙烯磺酰氯树脂功能基团的均一性
Determination of glyphosate in soil by high performance liquid chromatography after derivatization with p-toluenesulphonyl chloride
对甲基苯磺酰氯衍生化液相色谱法测定土壤中草甘膦
N-acetylsulfanilyl chloride
Ｎ－乙酰基磺胺酰氯
sodium p--toluenesulfonchloramide trihydrate
三水合甲苯磺酸氯醛甲酰胺钠
Rapid determination of 4-amino-6-chlorobenzene-1-3-disulphonamide
4-氨基-6氯苯-1,3-二磺酰胺含量的快速测定
Catalyst Oxidation of 2-Chloro-4-methylsulfonyl-toluene in Liquid-phase
液相催化氧化合成2-氯-4-甲磺酰基苯甲酸
Studies on Design Synthesis and Herbicidal Activity of N-(Chloronictinic) O-substituent Aryl Sulfonamides;
N-（氯烟酰基）邻取代基芳基磺酰胺的设计合成及除草活性的研究
Preparation methods for synthesis of sulfated polysaccharides by chlorosulfonic acid-pyridine method and chlorosulfonic acid-methanamide method were detailed.
重点介绍了氯磺酸－吡啶法和氯磺酸－甲酰胺法制备硫酸化多糖的情况。
Synthesis of Methyl 4-Chloro-2-(N-methyl-N-phenylsulphonamide)benzoate
4-氯-2-(N-甲基-N-苯基胺磺酰基)苯甲酸甲酯的合成